7B1V
DtxR-like iron-dependent regulator IdeR complexed with cobalt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-01-26 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97950 |
Spacegroup name | P 1 |
Unit cell lengths | 43.888, 45.564, 66.275 |
Unit cell angles | 109.12, 93.20, 113.98 |
Refinement procedure
Resolution | 61.100 - 2.040 |
R-factor | 0.2335 |
Rwork | 0.232 |
R-free | 0.26180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1u8r |
RMSD bond length | 0.002 |
RMSD bond angle | 1.149 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.100 | 2.220 |
High resolution limit [Å] | 2.040 | 2.040 |
Rmerge | 0.058 | 0.579 |
Rmeas | 0.069 | 0.748 |
Rpim | 0.037 | 0.465 |
Number of reflections | 17216 | 862 |
<I/σ(I)> | 10.3 | 1.5 |
Completeness [%] | 83.5 | 54.2 |
Redundancy | 3.3 | 2.4 |
CC(1/2) | 0.997 | 0.658 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 25%(w/v) PEG 1500 |