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7B1J

Orthorhombic P21212 Structure of Human Mad1 C-terminal Domain in Complex with Phosphorylated Bub1 CD1 Domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2020-07-21
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.9795
Spacegroup nameP 21 21 2
Unit cell lengths87.680, 133.980, 34.750
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution34.750 - 2.900
R-factor0.263
Rwork0.261
R-free0.29610
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4dzo
RMSD bond length0.025
RMSD bond angle2.330
Data reduction softwarexia2
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]34.7503.500
High resolution limit [Å]2.9002.900
Rmerge0.0330.469
Rmeas0.0360.510
Rpim0.0140.020
Number of reflections9638454
<I/σ(I)>25.93.9
Completeness [%]100.099.6
Redundancy3.63.6
CC(1/2)1.0000.977
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP29310% Isopropanol, 0.1 M Na HEPES, pH 7.5, 20% PEG 4000

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