7AZW
Crystal structure of the MIZ1-BTB-domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-08-28 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.03320 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 48.788, 34.518, 172.564 |
Unit cell angles | 90.00, 96.18, 90.00 |
Refinement procedure
Resolution | 35.170 - 2.100 |
R-factor | 0.2411 |
Rwork | 0.239 |
R-free | 0.28290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3m52 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.050 | 2.160 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.130 | 1.079 |
Number of reflections | 17046 | 1417 |
<I/σ(I)> | 7.4 | |
Completeness [%] | 99.8 | |
Redundancy | 4.5 | |
CC(1/2) | 0.996 | 0.789 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | PEG 4000, sodium acetate |