7AYP
Structure of a GH11 domain refined from the X-ray diffraction data of a GH11-CBM36-1 crystal.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-12-14 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.65 |
| Spacegroup name | P 63 |
| Unit cell lengths | 108.216, 108.216, 54.228 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 54.108 - 1.700 |
| R-factor | 0.171746959432 |
| Rwork | 0.171 |
| R-free | 0.18689 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2dcj |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.934 |
| Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 93.690 | 3.900 |
| High resolution limit [Å] | 1.470 | 1.470 |
| Number of reflections | 65364 | 3225 |
| <I/σ(I)> | 15.81 | |
| Completeness [%] | 99.9 | 99 |
| Redundancy | 1 | |
| CC(1/2) | 0.999 | 0.814 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 293.16 | Na acetate, (NH4)2SO4 |
