7AYP

Structure of a GH11 domain refined from the X-ray diffraction data of a GH11-CBM36-1 crystal.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-12-14
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.65
Spacegroup name	P 63
Unit cell lengths	108.216, 108.216, 54.228
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	54.108 - 1.700
R-factor	0.171746959432
Rwork	0.171
R-free	0.18689
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2dcj
RMSD bond length	0.006
RMSD bond angle	0.934
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	93.690	3.900
High resolution limit [Å]	1.470	1.470
Number of reflections	65364	3225
<I/σ(I)>	15.81
Completeness [%]	99.9	99
Redundancy	1
CC(1/2)	0.999	0.814

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.8	293.16	Na acetate, (NH4)2SO4