7AX5
Anammox-specific acyl carrier protein from Kuenenia stuttgartiensis; ensemble refinement
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-28 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 64 |
Unit cell lengths | 76.810, 76.810, 30.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.404 - 1.756 |
R-factor | 0.1776 |
Rwork | 0.175 |
R-free | 0.23430 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.ensemble_refinement:1.15.2_3472)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.404 | 1.900 |
High resolution limit [Å] | 1.756 | 1.760 |
Rpim | 0.025 | 0.652 |
Number of reflections | 7492 | 1132 |
<I/σ(I)> | 16.4 | |
Completeness [%] | 91.6 | |
Redundancy | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 28% (v/v) PEG 400, 200 mM calcium acetate, 100 mM sodium acetate pH 4.5 and 10 mM zinc chloride |