7ALT
Structure of Drosophila Serrate C2-DSL-EGF1-EGF2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.329, 49.402, 93.123 |
Unit cell angles | 90.00, 110.25, 90.00 |
Refinement procedure
Resolution | 45.610 - 2.030 |
R-factor | 0.222 |
Rwork | 0.220 |
R-free | 0.25790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5mw7 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.811 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_3965) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.610 | 2.103 |
High resolution limit [Å] | 2.030 | 2.030 |
Number of reflections | 38729 | 3814 |
<I/σ(I)> | 11.1 | |
Completeness [%] | 98.9 | |
Redundancy | 3.3 | |
CC(1/2) | 0.998 | 0.769 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 290 | 0.1M imidazole malate pH 7, 25% PEG4K |