7ALM
Crystal structure of human GDAP1 at 2.8 Angstrom resolution.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2019-03-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.808, 115.878, 116.595 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.360 - 2.800 |
R-factor | 0.2436 |
Rwork | 0.243 |
R-free | 0.26150 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.462 |
Data reduction software | XDS (Jan 31, 2020) |
Data scaling software | Aimless (0.7.4) |
Phasing software | CRANK2 |
Refinement software | PHENIX (1.18_3861) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.360 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.040 | 0.362 |
Rmeas | 0.056 | 0.512 |
Rpim | 0.040 | 0.362 |
Number of reflections | 24883 | 3571 |
<I/σ(I)> | 11.55 | 2.04 |
Completeness [%] | 99.6 | 100 |
Redundancy | 2 | 2 |
CC(1/2) | 0.997 | 0.854 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M Magnesium formate, 20 % PEG3350 |