7AJP

Crystal Structure of Human Adenovirus 56 Fiber Knob

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-06
Detector	DECTRIS PILATUS 2M
Wavelength(s)	1.00
Spacegroup name	C 1 2 1
Unit cell lengths	132.443, 182.529, 117.029
Unit cell angles	90.00, 118.54, 90.00

Refinement procedure

Resolution	42.645 - 1.382
R-factor	0.134641935546
Rwork	0.134
R-free	0.16687
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1uxe
RMSD bond length	0.010
RMSD bond angle	1.086
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.100	1.460
High resolution limit [Å]	1.380	1.380
Rmeas	0.086	1.461
Number of reflections	491039	80171
<I/σ(I)>	12.41	1.15
Completeness [%]	98.9	97
Redundancy	6.8	6.5
CC(1/2)	0.999	0.479

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.4	277	20 % PEG3350, 200 mM magnesium nitrate hexahydrate