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7AIA

Complex of human GDAP1 with hexadecanedioic acid

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2019-12-08
DetectorDECTRIS EIGER2 XE 16M
Wavelength(s)0.9795
Spacegroup nameP 21 21 21
Unit cell lengths73.045, 114.914, 116.866
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution45.629 - 2.200
Rwork0.202
R-free0.22990
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)GDAP1
RMSD bond length0.014
RMSD bond angle1.790
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0267)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.6302.279
High resolution limit [Å]2.2002.200
Number of reflections505254965
<I/σ(I)>12.72
Completeness [%]99.7
Redundancy6.6
CC(1/2)0.9980.657
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2770.2 M Lithium sulfate, 0.1 M bis-Tris pH 5.5, 25% w/v PEG 3350

222624

PDB entries from 2024-07-17

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