Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-02-10 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 113.954, 39.592, 90.517 |
| Unit cell angles | 90.00, 104.96, 90.00 |
Refinement procedure
| Resolution | 55.050 - 1.760 |
| Rwork | 0.189 |
| R-free | 0.22390 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | internal |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.225 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.050 | 1.823 |
| High resolution limit [Å] | 1.760 | 1.760 |
| Rmerge | 0.501 | |
| Number of reflections | 38875 | 3853 |
| <I/σ(I)> | 19.61 | |
| Completeness [%] | 99.2 | |
| Redundancy | 3.3 | |
| CC(1/2) | 0.999 | 0.805 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 22% PEG1500, 0.2M MES pH 6.0 |
