7A9P
Racemic compound of RNA duplexes.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.277 |
Spacegroup name | P 1 |
Unit cell lengths | 21.231, 26.617, 38.935 |
Unit cell angles | 105.60, 97.71, 90.81 |
Refinement procedure
Resolution | 37.114 - 1.985 |
Rwork | 0.235 |
R-free | 0.32630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6zq9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.631 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.200 | 2.110 |
High resolution limit [Å] | 1.985 | 1.985 |
Rmeas | 0.118 | 0.302 |
Number of reflections | 5085 | 782 |
<I/σ(I)> | 7.74 | 3.72 |
Completeness [%] | 90.4 | |
Redundancy | 3.6 | |
CC(1/2) | 0.991 | 0.962 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.2 M zinc acetate, 0.1 M cacodylate buffer, 18% w/v polyethylene glycol 8000. |