7A9C
Human serum albumin (HSA) crystallized in the presence of yttrium (III) chloride
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2009-12-04 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.7 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 55.270, 71.930, 180.130 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.002 - 2.750 |
| Rwork | 0.238 |
| R-free | 0.29460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bxi |
| RMSD bond length | 0.002 |
| RMSD bond angle | 1.203 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0232 2018/13/08) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.820 |
| High resolution limit [Å] | 2.750 | 2.750 |
| Number of reflections | 35814 | 2442 |
| <I/σ(I)> | 16.8 | |
| Completeness [%] | 99.5 | 93.8 |
| Redundancy | 16.2 | |
| CC(1/2) | 0.999 | 0.641 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | 2mM yttrium chloride |
