7A8O
rsGreen0.7-K206A-N205S in the green-on state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-19 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 102.640, 102.640, 50.304 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.344 - 1.600 |
R-factor | 0.1626 |
Rwork | 0.161 |
R-free | 0.20120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4xow |
Data reduction software | XDS |
Data scaling software | Aimless (0.6.2) |
Phasing software | PHASER (2.7.16) |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 45.900 | 45.900 | 1.630 |
High resolution limit [Å] | 1.600 | 8.760 | 1.600 |
Rmerge | 0.091 | 0.049 | 0.684 |
Rmeas | 0.098 | 0.053 | 0.730 |
Rpim | 0.034 | 0.020 | 0.250 |
Total number of observations | 281204 | 1870 | 14240 |
Number of reflections | 36042 | 276 | 1764 |
<I/σ(I)> | 12.8 | 29.1 | 2.6 |
Completeness [%] | 100.0 | 99.2 | 100 |
Redundancy | 7.8 | 6.8 | 8.1 |
CC(1/2) | 0.998 | 0.995 | 0.874 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 200 mM Maic acid pH 7.0 20 % PEG 3350 |