7A8J
rsGreen0.7-K206A-H148V in the green-on state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-18 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | H 3 2 |
Unit cell lengths | 140.616, 140.616, 73.004 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.592 - 1.850 |
R-factor | 0.1912 |
Rwork | 0.189 |
R-free | 0.23150 |
RMSD bond length | 0.009 |
RMSD bond angle | 0.956 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.23) |
Phasing software | PHENIX (1.11) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.760 | 46.760 | 1.890 |
High resolution limit [Å] | 1.850 | 9.060 | 1.850 |
Rmerge | 0.051 | 0.018 | 0.664 |
Rmeas | 0.053 | 0.020 | 0.699 |
Rpim | 0.017 | 0.006 | 0.217 |
Total number of observations | 241673 | ||
Number of reflections | 23673 | 224 | 1443 |
<I/σ(I)> | 28.4 | ||
Completeness [%] | 100.0 | 99.1 | 100 |
Redundancy | 10.2 | 9.9 | 10.3 |
CC(1/2) | 1.000 | 1.000 | 0.932 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM MES pH 6.5 25 % PEG 550 mme 10 mM ZnSO4 |