7A8D
rsGreen0.7-K206A-F165W partially in the green-on state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-18 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | H 3 2 |
Unit cell lengths | 140.570, 140.570, 72.972 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.742 - 1.650 |
R-factor | 0.1933 |
Rwork | 0.192 |
R-free | 0.21910 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.905 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHENIX (1.11) |
Refinement software | PHENIX (1.11) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.740 | 46.740 | 1.680 |
High resolution limit [Å] | 1.650 | 9.040 | 1.650 |
Rmerge | 0.044 | 0.042 | 0.748 |
Rmeas | 0.046 | 0.045 | 0.785 |
Rpim | 0.014 | 0.014 | 0.238 |
Total number of observations | 371129 | 2438 | 17525 |
Number of reflections | 33227 | 229 | 1624 |
<I/σ(I)> | 27.7 | 80.5 | 3.2 |
Completeness [%] | 100.0 | 99.4 | 100 |
Redundancy | 11.2 | 10.6 | 10.8 |
CC(1/2) | 0.999 | 0.997 | 0.894 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 200 mM NH4F 20 % PEG 3350 |