7A87
rsGreen0.7-K206A-F145M in the green-on state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-23 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | H 3 2 |
Unit cell lengths | 139.313, 139.313, 72.455 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.360 - 1.750 |
R-factor | 0.1934 |
Rwork | 0.192 |
R-free | 0.22770 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.842 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.15) |
Phasing software | PHASER (2.6.0) |
Refinement software | PHENIX (1.11) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.360 | 46.360 | 1.780 |
High resolution limit [Å] | 1.750 | 9.090 | 1.750 |
Rmerge | 0.052 | 0.027 | 0.699 |
Rmeas | 0.055 | 0.029 | 0.734 |
Rpim | 0.017 | 0.009 | 0.222 |
Total number of observations | 276606 | 2118 | 15638 |
Number of reflections | 27188 | 217 | 1478 |
<I/σ(I)> | 25.8 | 74.9 | 3.8 |
Completeness [%] | 100.0 | 99.4 | 99.8 |
Redundancy | 10.2 | 9.8 | 10.6 |
CC(1/2) | 1.000 | 1.000 | 0.901 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM Bis-tris pH 6.5 20 % PEG 1500 |