7A7R
rsGreenF-K206A in the green-off state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-28 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9801 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 106.185, 106.185, 35.907 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.487 - 2.350 |
R-factor | 0.1774 |
Rwork | 0.174 |
R-free | 0.24320 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.001 |
RMSD bond angle | 0.459 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHENIX (1.11) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.490 | 47.490 | 2.430 |
High resolution limit [Å] | 2.350 | 9.100 | 2.350 |
Rmerge | 0.146 | 0.062 | 0.667 |
Rmeas | 0.152 | 0.067 | 0.695 |
Rpim | 0.043 | 0.022 | 0.196 |
Total number of observations | 1847 | 11045 | |
Number of reflections | 9057 | 199 | 870 |
<I/σ(I)> | 16.3 | 28.2 | 4.7 |
Completeness [%] | 100.0 | 99.5 | 100 |
Redundancy | 12.4 | 9.3 | 12.7 |
CC(1/2) | 0.997 | 0.995 | 0.915 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 200 mM NaCl 100 mM MES pH 6.0 20 % PEG 6000 |