7A67
Pcc1Pcc2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-14 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.980066 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 69.898, 69.898, 92.751 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.950 - 3.180 |
R-factor | 0.192 |
Rwork | 0.185 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3enc |
RMSD bond length | 0.010 |
RMSD bond angle | 1.250 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 34.950 | 34.950 | 3.360 |
High resolution limit [Å] | 3.170 | 9.240 | 3.170 |
Rmerge | 0.212 | 0.070 | 1.796 |
Rmeas | 0.218 | 0.073 | 1.847 |
Total number of observations | 87363 | ||
Number of reflections | 4659 | 219 | 678 |
<I/σ(I)> | 10.93 | 37.93 | 1.54 |
Completeness [%] | 98.4 | 98.2 | 91 |
Redundancy | 18.751 | 17.301 | 17.488 |
CC(1/2) | 0.997 | 0.998 | 0.859 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 15% PEG 6000 and 5% glycerol |