7ZC9
Human Pikachurin/EGFLAM C-terminal Laminin-G domain (LG3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-04-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.976 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 73.805, 103.818, 133.534 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.380 - 2.100 |
R-factor | 0.2085 |
Rwork | 0.207 |
R-free | 0.24590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sh4 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.644 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.380 | 2.160 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.098 | 1.276 |
Rpim | 0.058 | 0.742 |
Number of reflections | 30331 | 2451 |
<I/σ(I)> | 11.9 | 1.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 7.6 |
CC(1/2) | 0.999 | 0.689 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 1.5-2.0 M ammonium sulfate 100 mM sodium acetate pH 4.6 |