7YLL

Crystal structure of TTEDbh

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-07-18
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97929
Spacegroup name	P 42 21 2
Unit cell lengths	105.196, 105.196, 74.211
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	14.877 - 2.600
R-factor	0.231538208837
Rwork	0.230
R-free	0.26531
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2rdi
RMSD bond length	0.008
RMSD bond angle	1.397
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Refinement software	PHENIX (1.12-2829_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	14.880	2.770
High resolution limit [Å]	2.600	2.600
Number of reflections	22314	2185
<I/σ(I)>	133.9
Completeness [%]	98.2
Redundancy	7.1
CC(1/2)	0.980	0.998

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	500 mM NaCl, 5 mM Mg3(PO4)2, 18% [w/v] PEG 3350