7Y6Z

RLGSGG-AtPRT6 UBR box (I222)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	193
Detector technology	PIXEL
Collection date	2019-11-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1
Spacegroup name	I 2 2 2
Unit cell lengths	38.986, 45.754, 86.824
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.670 - 1.598
R-factor	0.238
Rwork	0.234
R-free	0.27140
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6lhn
RMSD bond length	0.019
RMSD bond angle	1.647
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.670	1.655
High resolution limit [Å]	1.598	1.598
Number of reflections	10003	571
<I/σ(I)>	26.829
Completeness [%]	93.3
Redundancy	6.2
CC(1/2)	0.997	0.865

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	0.2 M Calcium acetate hydrate, 20% (w/v) PEG 3350