7W3N
Crystal structure of Ufm1 fused to UFBP1 UFIM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-04 |
Detector | RIGAKU HyPix-6000HE |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 53.411, 53.411, 82.231 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.414 - 1.600 |
R-factor | 0.182 |
Rwork | 0.181 |
R-free | 0.20020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5hkh |
RMSD bond length | 0.015 |
RMSD bond angle | 1.426 |
Data reduction software | CrysalisPro |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.414 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.034 | 0.478 |
Number of reflections | 18508 | 1850 |
<I/σ(I)> | 34.9 | |
Completeness [%] | 100.0 | |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 28% 2-propanol, 3% PEG 200, 0.1M MES at pH 6.0 |