7VKK
Crystal structure of D. melanogaster SAMTOR V66W/E67P mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | I 2 3 |
Unit cell lengths | 168.494, 168.494, 168.494 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.680 - 3.550 |
R-factor | 0.2279 |
Rwork | 0.226 |
R-free | 0.27480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7vkr |
RMSD bond length | 0.007 |
RMSD bond angle | 1.198 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0123) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.680 | 3.680 |
High resolution limit [Å] | 3.550 | 3.550 |
Rmerge | 0.168 | 0.813 |
Number of reflections | 9792 | 950 |
<I/σ(I)> | 7.9 | 1.5 |
Completeness [%] | 99.8 | |
Redundancy | 6 | |
CC(1/2) | 0.992 | 0.686 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 5 | 290 | 1.8 M Ammonium sulfate, 0.1 M Bis-Tris, pH 6.5, and 2% (v/v) PEG monomethyl ether 550 |