7ULO
Potato leafroll virus N-terminal readthrough domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-21 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 63.229, 65.147, 109.681 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.010 - 2.210 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.23920 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.020 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.23) |
Phasing software | SHELXDE |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 65.150 | 65.150 | 2.290 |
High resolution limit [Å] | 2.210 | 8.850 | 2.210 |
Rmerge | 0.097 | 0.069 | 0.850 |
Rmeas | 0.107 | 0.076 | 1.103 |
Rpim | 0.045 | 0.031 | 0.693 |
Total number of observations | 115339 | 2022 | 3184 |
Number of reflections | 22427 | 403 | 1558 |
<I/σ(I)> | 10.5 | 27.4 | 0.8 |
Completeness [%] | 96.8 | 95.3 | 75.2 |
Redundancy | 5.1 | 5 | 2 |
CC(1/2) | 0.996 | 0.997 | 0.352 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293.15 | 0.1 M Tris-HCl, pH 8.5, 0.25 M ammonium sulfate, 14% PEG8000, 3% ethylene glycol, 5 mM DTT |