7U57

apo-CTX-M-15

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.1
Synchrotron site	ALS
Beamline	5.0.1
Temperature [K]	80
Detector technology	PIXEL
Collection date	2020-12-18
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	171.079, 51.033, 106.863
Unit cell angles	90.00, 112.59, 90.00

Refinement procedure

Resolution	51.710 - 2.370
R-factor	0.226
Rwork	0.222
R-free	0.32680
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4hbt
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.19.1_4122)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	51.710	9.000	1.760
High resolution limit [Å]	1.730	4.690	1.730
Rmerge		1.226
Number of reflections	74931	71	1
<I/σ(I)>	2
Completeness [%]	75.0
Redundancy	1.2	1.2	1
CC(1/2)	0.935	0.313	0.935

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.8	293	300 mM Ammonium sulfate, 30% PEG 4000