7TTL

Stable-5-LOX elongated Ha2 (4 copies ASU)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-16
Detector	DECTRIS EIGER2 X 16M
Wavelength(s)	0.9795
Spacegroup name	P 1 21 1
Unit cell lengths	76.791, 204.547, 106.768
Unit cell angles	90.00, 109.03, 90.00

Refinement procedure

Resolution	102.270 - 2.430
R-factor	0.2158
Rwork	0.215
R-free	0.27480
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3o8y
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	102.270	2.517
High resolution limit [Å]	2.430	2.430
Number of reflections	217327	11353
<I/σ(I)>	8.58	1.16
Completeness [%]	97.9
Redundancy	3.5
CC(1/2)	0.996	0.629

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	295	10% Tacsimate