7TLN

STRUCTURAL ANALYSIS OF THE INHIBITION OF THERMOLYSIN BY AN ACTIVE-SITE-DIRECTED IRREVERSIBLE INHIBITOR

Replaces:  6TLN

Experimental procedure

Spacegroup name	P 61 2 2
Unit cell lengths	94.200, 94.200, 131.400
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.300
Rwork	0.170
RMSD bond length	0.021 *
RMSD bond angle	2.900 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.300 *
Number of reflections	12268 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	2	calcium acetate	0.01 (M)
2	1	2	Tris acetate	0.01 (M)
3	1	2	dimethylsulfoxide	5 (%(v/v))	or 7%(v/v)