7T19
Rev1 Ternary Complex with dGTP and Ca2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-01-13 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.183, 73.599, 117.098 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.590 - 2.010 |
R-factor | 0.1864 |
Rwork | 0.181 |
R-free | 0.24220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6x6z |
RMSD bond length | 0.009 |
RMSD bond angle | 1.053 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.060 |
High resolution limit [Å] | 2.010 | 2.030 |
Number of reflections | 36239 | 1772 |
<I/σ(I)> | 6.87 | |
Completeness [%] | 99.5 | |
Redundancy | 4.4 | |
CC(1/2) | 0.993 | 0.443 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 15-23% PEG3350, 200 mM ammonium nitrate |