7S7Q
Heterodimeric complex of Pf12 and Pf41 of Plasmodium falciparum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-04-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.953644 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 73.712, 73.712, 332.241 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.355 | 49.355 | 3.020 |
High resolution limit [Å] | 2.850 | 8.430 | 2.850 |
Rmerge | 0.076 | 0.039 | 1.044 |
Rmeas | 0.081 | 0.041 | 1.117 |
Total number of observations | 322715 | ||
Number of reflections | 40863 | 1578 | 6458 |
<I/σ(I)> | 15.59 | 46.07 | 1.54 |
Completeness [%] | 99.7 | 99.1 | 98.2 |
Redundancy | 7.897 | 7.421 | 7.952 |
CC(1/2) | 0.999 | 0.999 | 0.849 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 281 | 10 mM cadmium chloride, 14% (w/v) PEG 4000, 25% glycerol, 50 mM HEPES pH 7.5 |