7RZ1

Hen egg-white lysozyme with ionic liquid ethanolammonium formate 14.4 mol%

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	CCD
Collection date	2018-05-02
Detector	ADSC QUANTUM 210r
Wavelength(s)	1.23980
Spacegroup name	P 43 21 2
Unit cell lengths	76.650, 76.650, 38.290
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	54.200 - 2.046
Rwork	0.160
R-free	0.24310
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	7jmu
RMSD bond length	0.010
RMSD bond angle	1.776
Data reduction software	iMOSFLM
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	54.200	2.100
High resolution limit [Å]	2.046	2.050
Number of reflections	7613	571
<I/σ(I)>	11.3	2.8
Completeness [%]	100.0	100
Redundancy	10.7
CC(1/2)	0.981	0.852

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	ethanolammonium formate 14.4mol% (ca. 50wt%) in water