7Q9A
MHC Class I A02 Allele presenting LLLGIGILVL, in complex with Mel5 TCR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-03-02 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97951 |
Spacegroup name | P 43 |
Unit cell lengths | 122.019, 122.019, 82.418 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.010 - 2.100 |
R-factor | 0.2064 |
Rwork | 0.204 |
R-free | 0.24320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hg1 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.676 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.020 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.105 | 2.600 |
Rmeas | 0.113 | 2.800 |
Rpim | 0.040 | 0.989 |
Number of reflections | 70731 | 3512 |
<I/σ(I)> | 10.6 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.7 | 7.8 |
CC(1/2) | 0.998 | 0.312 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.1M TRIS, 15% PEG 8000, 15% Glycerol, pH 7.5 |