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7Q5C

Crystal structure of OmpG in space group 96

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 2
Synchrotron siteSOLEIL
BeamlinePROXIMA 2
Temperature [K]100
Detector technologyPIXEL
Collection date2019-03-31
DetectorDECTRIS EIGER X 9M
Wavelength(s)0.97918
Spacegroup nameP 43 21 2
Unit cell lengths71.343, 71.343, 200.464
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution67.304 - 2.717
Rwork0.274
R-free0.32800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2iwv
RMSD bond length0.009
RMSD bond angle1.858
Data reduction softwarexia2
Data scaling softwareXDS
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0258)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]67.3042.788
High resolution limit [Å]2.7172.717
Rmeas0.0250.830
Number of reflections14670980
<I/σ(I)>16.9
Completeness [%]99.7
Redundancy2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION5.629430-60 mM Sodium Citrate, 50-70mM NaCl, 12-14 % (w/v) PEG-3350, 60-65 mM n-octyl-beta-d-glucoside, 6-12 mg/mL protein

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