7Q0Z
Crystal structure of CTX-M-14
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-20 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9762 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 41.361, 62.497, 86.421 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 23.960 - 1.000 |
| R-factor | 0.1602 |
| Rwork | 0.160 |
| R-free | 0.17190 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6gth |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.105 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.880 | 1.040 |
| High resolution limit [Å] | 1.000 | 1.000 |
| Rmeas | 0.038 | 0.247 |
| Number of reflections | 121023 | 11775 |
| <I/σ(I)> | 36.49 | 7.83 |
| Completeness [%] | 99.6 | |
| Redundancy | 12.1 | |
| CC(1/2) | 1.000 | 0.982 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 291 | 30 % PEG8000, 0.2 M lithium sulfate, 0.1 M sodium acetate |
