7PVN
Crystal Structure of Human UBA6 in Complex with ATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-12-19 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9762 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 123.949, 113.748, 183.537 |
Unit cell angles | 90.00, 96.49, 90.00 |
Refinement procedure
Resolution | 19.980 - 2.710 |
R-factor | 0.2341 |
Rwork | 0.233 |
R-free | 0.26170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cmm |
RMSD bond length | 0.005 |
RMSD bond angle | 0.873 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.710 | 2.710 |
Rmerge | 0.294 | 2.570 |
Rpim | 0.123 | 1.158 |
Number of reflections | 49253 | 986 |
<I/σ(I)> | 6 | 0.92 |
Completeness [%] | 72.5 | 21.8 |
Redundancy | 6.66 | 5.56 |
CC(1/2) | 0.985 | 0.170 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M Na-cacodylate, 0.16 M Ca-acetate, 15% PEG 8000 and 16% Glycerol |