7PC9
The PDZ domain of SYNJ2BP complexed with the PDZ-binding motif of HTLV1-TAX1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-03-17 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.990, 99.850, 173.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.327 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmeas | 0.316 | 2.430 |
Number of reflections | 41356 | 2991 |
<I/σ(I)> | 8.93 | 1.22 |
Completeness [%] | 99.3 | |
Redundancy | 13.46 | |
CC(1/2) | 0.995 | 0.449 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M HEPES pH 7.5, 10% w/v PEG 8000, 8% v/v Ethylene glycol |