Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2016-10-24 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.9794 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 124.127, 172.530, 159.710 |
Unit cell angles | 90.00, 104.53, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.500 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmeas | 0.230 | 0.950 |
Number of reflections | 129715 | 20801 |
<I/σ(I)> | 10.37 | 2.21 |
Completeness [%] | 99.8 | |
Redundancy | 7.06 | |
CC(1/2) | 0.990 | 0.720 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 0.2 M trimethanolamine N-oxide, 0.1 M Tris (pH 8.5), 20% PEG 2000 |