7OX3
Fab 6D3: hIL-9 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-25 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 60.480, 81.860, 116.540 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.640 | 1.800 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 63819 | 10037 |
<I/σ(I)> | 21.59 | |
Completeness [%] | 99.2 | |
Redundancy | 13.4 | |
CC(1/2) | 0.999 | 0.703 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.8 | 293 | 0.1M ammonium sulfate, 0.1M Tris, 16% PEG 1500, pH 5.8 |