7OIY

Crystal structure of the ZUFSP family member Mug105

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID30B
Synchrotron site	ESRF
Beamline	ID30B
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-01-28
Detector	DECTRIS EIGER R 4M
Wavelength(s)	0.967700
Spacegroup name	P 41
Unit cell lengths	88.235, 88.235, 111.011
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.460 - 2.050
R-factor	0.1738
Rwork	0.173
R-free	0.20390
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6ei1
RMSD bond length	0.003
RMSD bond angle	0.500
Data reduction software	XDS (20180126)
Data scaling software	XDS (20180126)
Phasing software	PHENIX
Refinement software	PHENIX (1.19.1_4122)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.460	2.124
High resolution limit [Å]	2.050	2.050
Number of reflections	53097	5246
<I/σ(I)>	10.35
Completeness [%]	99.8
Redundancy	6
CC(1/2)	0.998	0.441

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	1.8 M sodium acetate pH 7.0; 0.1 M BIS-TRIS propane pH 7.0