7NUG
Influenza A/California/07/2009(H1N1) endonuclease in complex with orientin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-08-25 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1.54187 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 74.361, 74.361, 126.462 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.150 - 1.900 |
R-factor | 0.1978 |
Rwork | 0.195 |
R-free | 0.25050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ya5 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.531 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.150 | 42.150 | 1.950 |
High resolution limit [Å] | 1.900 | 8.500 | 1.900 |
Rmerge | 0.089 | 0.033 | 1.192 |
Rmeas | 0.094 | 0.034 | 1.309 |
Total number of observations | 157145 | ||
Number of reflections | 16879 | 240 | 1211 |
<I/σ(I)> | 15.29 | 60.59 | 1.6 |
Completeness [%] | 99.5 | 96 | 99.3 |
Redundancy | 9.31 | 15.033 | 6.192 |
CC(1/2) | 0.998 | 1.000 | 0.582 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291.15 | MDP, PEG 1000, PEG 3350, Sodium HEPES, MOPS (acid), Magnesium chloride, Calcium chloride |