7NPC
ROR(gamma)t ligand binding domain in complex with allosteric ligand FM156
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.033210 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 107.603, 107.603, 100.205 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 53.860 - 1.470 |
R-factor | 0.16977 |
Rwork | 0.168 |
R-free | 0.19670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6sal |
RMSD bond length | 0.006 |
RMSD bond angle | 1.320 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.240 | 1.500 |
High resolution limit [Å] | 1.470 | 1.470 |
Number of reflections | 58535 | 2855 |
<I/σ(I)> | 25.7 | |
Completeness [%] | 100.0 | |
Redundancy | 113.1 | |
CC(1/2) | 1.000 | 0.382 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.5 | 293.15 | 1.6 M AmSO4, 0.1 M Tris |