7NJI
HEX1 (in cellulo) loaded on HARE serial crystallography chip
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2019-05-01 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 58.900, 58.900, 193.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 51.010 - 2.300 |
R-factor | 0.2212 |
Rwork | 0.219 |
R-free | 0.26010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1khi |
RMSD bond length | 0.010 |
RMSD bond angle | 1.157 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.940 | 2.382 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 9522 | 917 |
<I/σ(I)> | 3.2 | |
Completeness [%] | 100.0 | |
Redundancy | 93 | |
CC(1/2) | 0.909 | 0.382 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | IN CELL | 300 | Grown inside Spodoptera frugiperda Sf9 insect cells |