7NJH
HEX1 (in cellulo) grown inside HARE serial crystallography chip
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2020-06-13 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 58.550, 58.550, 192.700 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.710 - 2.500 |
R-factor | 0.2219 |
Rwork | 0.220 |
R-free | 0.25530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1khi |
RMSD bond length | 0.007 |
RMSD bond angle | 0.878 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.100 | 50.710 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 7394 | 706 |
<I/σ(I)> | 3.1 | |
Completeness [%] | 99.9 | |
Redundancy | 37 | |
CC(1/2) | 0.836 | 0.688 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | IN CELL | 300 | Transfected and grown in Spodoptera frugiperda Sf9 insect cells |