7NFQ

Fujian capmidlink domain in complex with Nb8193

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-05-14
Detector	DECTRIS EIGER2 X 16M
Wavelength(s)	0.9762
Spacegroup name	P 1 21 1
Unit cell lengths	42.583, 106.543, 98.405
Unit cell angles	90.00, 98.01, 90.00

Refinement procedure

Resolution	44.310 - 1.680
R-factor	0.1693
Rwork	0.167
R-free	0.20540
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6s5v
RMSD bond length	0.013
RMSD bond angle	1.209
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.18rc2_3794)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.310	1.743
High resolution limit [Å]	1.680	1.680
Number of reflections	69149	767
<I/σ(I)>	23.17
Completeness [%]	70.3
Redundancy	2
CC(1/2)	1.000	0.292

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	20% w/v PEG3350 and 0.2 M (NH4)2 citrate