7N91
P70 S6K1 IN COMPLEX WITH MSC2317067A-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-03-25 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.300, 74.550, 150.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.520 - 3.000 |
Rwork | 0.212 |
R-free | 0.27180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a60 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | CNX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.520 | 3.170 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.148 | 0.522 |
Rmeas | 0.168 | 0.564 |
Number of reflections | 13883 | 2106 |
<I/σ(I)> | 11.5 | 2.86 |
Completeness [%] | 96.1 | 95.8 |
Redundancy | 5.87 | 5.49 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 295 | 0.2M Bis-Tris pH 5.5, 0.1M Li2SO4, 26-28% PEG3350 |