7N2L
MicroED structure of a mutant mammalian prion segment
Experimental procedure
Spacegroup name | P 1 |
Unit cell lengths | 4.870, 10.060, 30.660 |
Unit cell angles | 94.85, 90.26, 99.99 |
Refinement procedure
Resolution | 7.980 - 0.900 |
R-factor | 0.1967 |
Rwork | 0.197 |
R-free | 0.19800 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 7.980 | 7.980 | 0.930 |
High resolution limit [Å] | 0.900 | 1.930 | 0.900 |
Rmerge | 0.197 | 0.151 | 0.475 |
Rmeas | 0.214 | 0.163 | 0.529 |
Total number of observations | 18502 | ||
Number of reflections | 3437 | 350 | 330 |
<I/σ(I)> | 5.21 | 8.61 | 2.56 |
Completeness [%] | 81.0 | 79 | 82.3 |
Redundancy | 5.383 | 5.834 | 4.858 |
CC(1/2) | 0.988 | 0.986 | 0.783 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |