7M0K
HPK1 IN COMPLEX WITH COMPOUND 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 |
Unit cell lengths | 45.074, 76.627, 89.200 |
Unit cell angles | 90.02, 97.02, 89.98 |
Refinement procedure
Resolution | 88.530 - 2.010 |
R-factor | 0.2483 |
Rwork | 0.248 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | previously solved structure |
RMSD bond length | 0.011 |
RMSD bond angle | 1.470 |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 88.530 | 2.260 |
High resolution limit [Å] | 2.010 | 2.010 |
Rmeas | 0.045 | 0.590 |
Number of reflections | 74742 | 21707 |
<I/σ(I)> | 12.37 | 2.15 |
Completeness [%] | 94.7 | 92.6 |
Redundancy | 2.2 | 2.2 |
CC(1/2) | 0.999 | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 7% PEG 5K MNE, 0.05 M HEPES pH 6.5, Na3Cit pH 7, 20 mM Tris pH 8.0 , 150 mM NaCl , 5% Glycerol |