7LP2
Structure of Nedd4L WW3 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-01-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9753 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 91.598, 91.598, 37.982 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.980 - 1.880 |
R-factor | 0.1896 |
Rwork | 0.185 |
R-free | 0.22790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2mpt |
RMSD bond length | 0.008 |
RMSD bond angle | 0.958 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.990 | 1.781 |
High resolution limit [Å] | 1.720 | 1.720 |
Rmerge | 0.023 | 0.590 |
Rmeas | 0.331 | 0.033 |
Number of reflections | 13684 | 1731 |
<I/σ(I)> | 20.61 | 1.22 |
Completeness [%] | 99.9 | 95.77 |
Redundancy | 2 | 2 |
CC(1/2) | 1.000 | 0.449 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 2.0M Ammonium Sulfate, 0.1M BIS-TRIS |