7KNW
Crystal structure of SND1 in complex with C-26-A2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | LIQUID ANODE |
| Source details | BRUKER METALJET |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-12-04 |
| Detector | Bruker PHOTON II |
| Wavelength(s) | 1.34 |
| Spacegroup name | P 1 |
| Unit cell lengths | 61.240, 86.154, 82.426 |
| Unit cell angles | 82.71, 72.00, 65.42 |
Refinement procedure
| Resolution | 30.000 - 2.650 |
| R-factor | 0.2674 |
| Rwork | 0.264 |
| R-free | 0.33760 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.503 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.720 |
| High resolution limit [Å] | 2.650 | 2.650 |
| Rmerge | 1.000 | 1.000 |
| Number of reflections | 38827 | 2497 |
| <I/σ(I)> | 5.1 | |
| Completeness [%] | 91.8 | 90.8 |
| Redundancy | 5.5 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293.15 | 0.1 M MES-NaOH pH 6.2, 1.0 M trisodium citrate |
