7JYO
JAK2 JH2 in complex with JAK064
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-12 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.568, 57.375, 61.071 |
Unit cell angles | 90.00, 111.00, 90.00 |
Refinement procedure
Resolution | 40.442 - 2.161 |
R-factor | 0.188225496472 |
Rwork | 0.185 |
R-free | 0.24640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5usz |
RMSD bond length | 0.007 |
RMSD bond angle | 0.805 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.240 |
High resolution limit [Å] | 2.160 | 2.160 |
Rmeas | 0.068 | 0.233 |
Rpim | 0.038 | 0.143 |
Number of reflections | 15316 | 1383 |
<I/σ(I)> | 15.2 | 2.95 |
Completeness [%] | 98.5 | 89.5 |
Redundancy | 3 | 2.1 |
CC(1/2) | 0.979 | 0.930 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277.15 | 0.1M TRIS, PH 8.0 0.2M SODIUM ACETATE, 0.001 M TCEP, 12-24% PEG 4,000 |