7JQR

Abeta 16-36 beta-hairpin mimic with E22G Arctic mutation

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	123.15
Detector technology	CCD
Collection date	2017-10-13
Detector	RIGAKU SATURN 944+
Wavelength(s)	1.54
Spacegroup name	P 41 3 2
Unit cell lengths	47.219, 47.219, 47.219
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.280 - 2.070
R-factor	0.208
Rwork	0.203
R-free	0.25410
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX (dev_3908)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.280	2.149
High resolution limit [Å]	2.070	2.075
Rmerge	0.012
Rmeas	0.017
Number of reflections	2070	126
<I/σ(I)>	65.87
Completeness [%]	99.4	100
Redundancy	90.7
CC(1/2)	1.000	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		297.15	calcium chloride, sodium acetate, isopropanol